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dc.creatorKarljiković-Rajić, Katarina
dc.creatorStanković, B
dc.creatorGranov, A
dc.creatorBinenfeld, Z.J.
dc.date.accessioned2019-09-02T10:47:06Z
dc.date.available2019-09-02T10:47:06Z
dc.date.issued1988
dc.identifier.issn0731-7085
dc.identifier.urihttps://farfar.pharmacy.bg.ac.rs/handle/123456789/43
dc.description.abstractPralidoxime chloride (PAM-2Cl) has been determined spectrophotometrically in Britton-Robinson buffer solution at pH = 6.45; the method is based on measurement of the absorbance of the Pd(II)-pralidoxime complex at 327 nm. Studies of the composition of the complex by Job's continuous variation method, the molar ratio method and Bent-French's method yielded a Pd(II):pralidoxime ratio of 1:1. The conditional stability constant (K′) of the complex at the optimum pH of 6.45 and an ionic strength (μ) of 0.3 M was found to be 105.2. The molar absorptivity was 1.05 × 104 1 mol-1 cm-1. Beer's law was obeyed at concentrations up to 60 μM. The detection limit was 0.55 μg ml-1. The relative standard deviation (N = 10) was 0.28-1.03%. The method was accurate and sensitive for the analysis of PAM-2Cl in water and tablets.en
dc.rightsrestrictedAccess
dc.sourceJournal of Pharmaceutical and Biomedical Analysis
dc.subjectcompleximetryen
dc.subjectpalladium(II) chlorideen
dc.subjectPralidoxime chlorideen
dc.subjectspectrophotometryen
dc.subjecttablets.en
dc.titleUse of palladium(II) chloride as colour-forming reagent in determination of pralidoxime chloride in water and tabletsen
dc.typearticle
dc.rights.licenseARR
dcterms.abstractГранов, A; Карљиковић-Рајић, Катарина; Биненфелд, З.Ј.; Станковић, Б;
dc.citation.volume6
dc.citation.issue6-8
dc.citation.spage773
dc.citation.epage780
dc.citation.other6(6-8): 773-780
dc.citation.rankM22
dc.identifier.doi10.1016/0731-7085(88)80090-6
dc.identifier.scopus2-s2.0-0023812587
dc.type.versionpublishedVersion


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Приказ основних података о документу