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Multi-analytical study of techniques and palettes of wall paintings of the monastery of Zica, Serbia

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2016
Authors
Holclajtner-Antunović, Ivanka
Stojanović-Marić, Milica
Bajuk-Bogdanović, Danica
Zikić, Radisa
Uskoković-Marković, Snežana
Article (Published version)
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Abstract
The present multi-analytical study concentrates on establishing the painting techniques and the identity of the wall painting materials used by the artists from the 13th and 14th centuries to decorate the Zica monastery, Serbia. For this purpose, we demonstrate that micro-Raman spectroscopy is an efficient, non-destructive method with high spatial resolution which gives molecular and crystal structural information of a wide variety of both inorganic and organic materials. It is shown that elementary composition revealed through scanning electron microscopy with energy dispersive X-ray spectroscopy and energy dispersive X-ray fluorescence spectroscopy is necessary in some cases to confirm the identity of pigments and binders identified by micro-Raman spectroscopy. It was found that a fresco technique, in combination with mainly natural earth pigments such as red ochre, yellow ochre and green earth, was used. Expensive natural pigment lapis lazuli was exclusively used for obtaining blue ...colour while pure vermilion was used by the artists from the first period of decorations at the beginning of the 13th century. A mixture of pigments was used for attaining different colour shades. For the gilding of saint's haloes, thin golden foil was deposited over the tin sheet. In order to get a desirable optical and aesthetical impression, the metallic leaves were deposited over the yellow ochre preparatory layer. Deposits of gypsum on wall paintings as well as traces of weddellite are degradation products formed as a result of exposing wall paintings to environmental conditions.

Source:
Spectroscopy Letters, 2016, 156, 78-88
Publisher:
  • Pergamon-Elsevier Science Ltd, Oxford
Funding / projects:
  • Urbanisation Processes and Development of Mediaeval Society (RS-177021)

DOI: 10.1016/j.saa.2015.11.031

ISSN: 1386-1425

PubMed: 26654964

WoS: 000369201200011

Scopus: 2-s2.0-84948699156
[ Google Scholar ]
18
16
URI
https://farfar.pharmacy.bg.ac.rs/handle/123456789/2586
Collections
  • Radovi istraživača / Researchers’ publications
Institution/Community
Pharmacy
TY  - JOUR
AU  - Holclajtner-Antunović, Ivanka
AU  - Stojanović-Marić, Milica
AU  - Bajuk-Bogdanović, Danica
AU  - Zikić, Radisa
AU  - Uskoković-Marković, Snežana
PY  - 2016
UR  - https://farfar.pharmacy.bg.ac.rs/handle/123456789/2586
AB  - The present multi-analytical study concentrates on establishing the painting techniques and the identity of the wall painting materials used by the artists from the 13th and 14th centuries to decorate the Zica monastery, Serbia. For this purpose, we demonstrate that micro-Raman spectroscopy is an efficient, non-destructive method with high spatial resolution which gives molecular and crystal structural information of a wide variety of both inorganic and organic materials. It is shown that elementary composition revealed through scanning electron microscopy with energy dispersive X-ray spectroscopy and energy dispersive X-ray fluorescence spectroscopy is necessary in some cases to confirm the identity of pigments and binders identified by micro-Raman spectroscopy. It was found that a fresco technique, in combination with mainly natural earth pigments such as red ochre, yellow ochre and green earth, was used. Expensive natural pigment lapis lazuli was exclusively used for obtaining blue colour while pure vermilion was used by the artists from the first period of decorations at the beginning of the 13th century. A mixture of pigments was used for attaining different colour shades. For the gilding of saint's haloes, thin golden foil was deposited over the tin sheet. In order to get a desirable optical and aesthetical impression, the metallic leaves were deposited over the yellow ochre preparatory layer. Deposits of gypsum on wall paintings as well as traces of weddellite are degradation products formed as a result of exposing wall paintings to environmental conditions.
PB  - Pergamon-Elsevier Science Ltd, Oxford
T2  - Spectroscopy Letters
T1  - Multi-analytical study of techniques and palettes of wall paintings of the monastery of Zica, Serbia
VL  - 156
SP  - 78
EP  - 88
DO  - 10.1016/j.saa.2015.11.031
ER  - 
@article{
author = "Holclajtner-Antunović, Ivanka and Stojanović-Marić, Milica and Bajuk-Bogdanović, Danica and Zikić, Radisa and Uskoković-Marković, Snežana",
year = "2016",
abstract = "The present multi-analytical study concentrates on establishing the painting techniques and the identity of the wall painting materials used by the artists from the 13th and 14th centuries to decorate the Zica monastery, Serbia. For this purpose, we demonstrate that micro-Raman spectroscopy is an efficient, non-destructive method with high spatial resolution which gives molecular and crystal structural information of a wide variety of both inorganic and organic materials. It is shown that elementary composition revealed through scanning electron microscopy with energy dispersive X-ray spectroscopy and energy dispersive X-ray fluorescence spectroscopy is necessary in some cases to confirm the identity of pigments and binders identified by micro-Raman spectroscopy. It was found that a fresco technique, in combination with mainly natural earth pigments such as red ochre, yellow ochre and green earth, was used. Expensive natural pigment lapis lazuli was exclusively used for obtaining blue colour while pure vermilion was used by the artists from the first period of decorations at the beginning of the 13th century. A mixture of pigments was used for attaining different colour shades. For the gilding of saint's haloes, thin golden foil was deposited over the tin sheet. In order to get a desirable optical and aesthetical impression, the metallic leaves were deposited over the yellow ochre preparatory layer. Deposits of gypsum on wall paintings as well as traces of weddellite are degradation products formed as a result of exposing wall paintings to environmental conditions.",
publisher = "Pergamon-Elsevier Science Ltd, Oxford",
journal = "Spectroscopy Letters",
title = "Multi-analytical study of techniques and palettes of wall paintings of the monastery of Zica, Serbia",
volume = "156",
pages = "78-88",
doi = "10.1016/j.saa.2015.11.031"
}
Holclajtner-Antunović, I., Stojanović-Marić, M., Bajuk-Bogdanović, D., Zikić, R.,& Uskoković-Marković, S.. (2016). Multi-analytical study of techniques and palettes of wall paintings of the monastery of Zica, Serbia. in Spectroscopy Letters
Pergamon-Elsevier Science Ltd, Oxford., 156, 78-88.
https://doi.org/10.1016/j.saa.2015.11.031
Holclajtner-Antunović I, Stojanović-Marić M, Bajuk-Bogdanović D, Zikić R, Uskoković-Marković S. Multi-analytical study of techniques and palettes of wall paintings of the monastery of Zica, Serbia. in Spectroscopy Letters. 2016;156:78-88.
doi:10.1016/j.saa.2015.11.031 .
Holclajtner-Antunović, Ivanka, Stojanović-Marić, Milica, Bajuk-Bogdanović, Danica, Zikić, Radisa, Uskoković-Marković, Snežana, "Multi-analytical study of techniques and palettes of wall paintings of the monastery of Zica, Serbia" in Spectroscopy Letters, 156 (2016):78-88,
https://doi.org/10.1016/j.saa.2015.11.031 . .

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