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Use of pralidoxime-Pd(II) complex for the spectrophotometric determination of the cholinesterase reactivator (PAM-2Cl) in the urine

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1990
Authors
Karljiković-Rajić, Katarina
Stanković, B.S
Article (Published version)
Metadata
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Abstract
A simple and rapid method for the spectrophotometric determination of pralidoxime chloride in urine, based on complex formation with palladium(II) without preliminary mineralization of the sample, is described. The proposed method is shown to be reproducible and in good agreement with a reference method, which involved spectrophotometric determination of corresponding oximate ions in ammonium hydroxide solution at 336 nm. Our results indicate that the proposed method is reliable, rapid and of sufficient sensitivity for pralidoxime chloride analysis in urine.
Keywords:
Antidote / Pralidoxime chloride / Pralidoxime-Pd(II) complex / Spectrophotometric determination / Urine
Source:
Clinica Chimica Acta, 1990, 193, 3, 119-124

DOI: 10.1016/0009-8981(90)90243-L

ISSN: 0009-8981

Scopus: 2-s2.0-0025259055
[ Google Scholar ]
3
URI
https://farfar.pharmacy.bg.ac.rs/handle/123456789/56
Collections
  • Radovi istraživača / Researchers’ publications
Institution/Community
Pharmacy
TY  - JOUR
AU  - Karljiković-Rajić, Katarina
AU  - Stanković, B.S
PY  - 1990
UR  - https://farfar.pharmacy.bg.ac.rs/handle/123456789/56
AB  - A simple and rapid method for the spectrophotometric determination of pralidoxime chloride in urine, based on complex formation with palladium(II) without preliminary mineralization of the sample, is described. The proposed method is shown to be reproducible and in good agreement with a reference method, which involved spectrophotometric determination of corresponding oximate ions in ammonium hydroxide solution at 336 nm. Our results indicate that the proposed method is reliable, rapid and of sufficient sensitivity for pralidoxime chloride analysis in urine.
T2  - Clinica Chimica Acta
T1  - Use of pralidoxime-Pd(II) complex for the spectrophotometric determination of the cholinesterase reactivator (PAM-2Cl) in the urine
VL  - 193
IS  - 3
SP  - 119
EP  - 124
DO  - 10.1016/0009-8981(90)90243-L
ER  - 
@article{
author = "Karljiković-Rajić, Katarina and Stanković, B.S",
year = "1990",
abstract = "A simple and rapid method for the spectrophotometric determination of pralidoxime chloride in urine, based on complex formation with palladium(II) without preliminary mineralization of the sample, is described. The proposed method is shown to be reproducible and in good agreement with a reference method, which involved spectrophotometric determination of corresponding oximate ions in ammonium hydroxide solution at 336 nm. Our results indicate that the proposed method is reliable, rapid and of sufficient sensitivity for pralidoxime chloride analysis in urine.",
journal = "Clinica Chimica Acta",
title = "Use of pralidoxime-Pd(II) complex for the spectrophotometric determination of the cholinesterase reactivator (PAM-2Cl) in the urine",
volume = "193",
number = "3",
pages = "119-124",
doi = "10.1016/0009-8981(90)90243-L"
}
Karljiković-Rajić, K.,& Stanković, B.S. (1990). Use of pralidoxime-Pd(II) complex for the spectrophotometric determination of the cholinesterase reactivator (PAM-2Cl) in the urine. in Clinica Chimica Acta, 193(3), 119-124.
https://doi.org/10.1016/0009-8981(90)90243-L
Karljiković-Rajić K, Stanković B. Use of pralidoxime-Pd(II) complex for the spectrophotometric determination of the cholinesterase reactivator (PAM-2Cl) in the urine. in Clinica Chimica Acta. 1990;193(3):119-124.
doi:10.1016/0009-8981(90)90243-L .
Karljiković-Rajić, Katarina, Stanković, B.S, "Use of pralidoxime-Pd(II) complex for the spectrophotometric determination of the cholinesterase reactivator (PAM-2Cl) in the urine" in Clinica Chimica Acta, 193, no. 3 (1990):119-124,
https://doi.org/10.1016/0009-8981(90)90243-L . .

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