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Determination of metal content in some herbal drugs - Empirical and chemometric approach

Authorized Users Only
2005
Authors
Ražić, Slavica
Onjia, Antonije
Đogo-Mračević, Svetlana
Slavković, Latinka
Popović, Aleksandar
Article (Published version)
Metadata
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Abstract
The concentrations of Cu, Zn, Mn, Fe, K, Ca, Mg, Al, Ba and B in 26 herbal drugs of special importance in phytopharmacywere studied. Flame atomic absorption and emission spectrometry (FAAS, FAES), as well as inductively coupled plasma atomic emission spectrometry (ICP-AES), were applied in this work. The whole procedure, from sample preparation, via dissolution, to measurements, was validated by using CRM (NIST 1573a-tomato leaves), and the obtained recovery values are in the range from 91 to 102%. Drug samples originated from medicinal plants cultivated in Serbia contained Cu (4.47-14.08 mg kg(-1)), Zn (8.4-54.5 mg kg(-1)), Mn (9-155 mg kg(-1)), Fe (47-546 mg kg(-1)), K (0.20-6.24%), Ca (0.18-1.84%), Mg (0.13-1.09%), Al (16-416 mg kg(-1)), Ba (11.70-84.83 mg kg(-1)) and B (5.1-118.7 mg kg(-1)). In order to get a better insight into the elemental patterns, a common chemometric approach to data evaluation was used. Four significant factors identified by principal component analysis (PCA...) were attributed partly to the significant influential sources and high mobility of some elements thus referring to potential anthropogenic contamination as well.

Keywords:
herbal drugs / trace elements / AAS / AES / chemometrics / PCA
Source:
Talanta, 2005, 67, 1, 233-239
Publisher:
  • Elsevier Science BV, Amsterdam

DOI: 10.1016/j.talanta.2005.03.023

ISSN: 0039-9140

PubMed: 18970161

WoS: 000230528500031

Scopus: 2-s2.0-21344461513
[ Google Scholar ]
83
65
URI
https://farfar.pharmacy.bg.ac.rs/handle/123456789/577
Collections
  • Radovi istraživača / Researchers’ publications
Institution/Community
Pharmacy
TY  - JOUR
AU  - Ražić, Slavica
AU  - Onjia, Antonije
AU  - Đogo-Mračević, Svetlana
AU  - Slavković, Latinka
AU  - Popović, Aleksandar
PY  - 2005
UR  - https://farfar.pharmacy.bg.ac.rs/handle/123456789/577
AB  - The concentrations of Cu, Zn, Mn, Fe, K, Ca, Mg, Al, Ba and B in 26 herbal drugs of special importance in phytopharmacywere studied. Flame atomic absorption and emission spectrometry (FAAS, FAES), as well as inductively coupled plasma atomic emission spectrometry (ICP-AES), were applied in this work. The whole procedure, from sample preparation, via dissolution, to measurements, was validated by using CRM (NIST 1573a-tomato leaves), and the obtained recovery values are in the range from 91 to 102%. Drug samples originated from medicinal plants cultivated in Serbia contained Cu (4.47-14.08 mg kg(-1)), Zn (8.4-54.5 mg kg(-1)), Mn (9-155 mg kg(-1)), Fe (47-546 mg kg(-1)), K (0.20-6.24%), Ca (0.18-1.84%), Mg (0.13-1.09%), Al (16-416 mg kg(-1)), Ba (11.70-84.83 mg kg(-1)) and B (5.1-118.7 mg kg(-1)). In order to get a better insight into the elemental patterns, a common chemometric approach to data evaluation was used. Four significant factors identified by principal component analysis (PCA) were attributed partly to the significant influential sources and high mobility of some elements thus referring to potential anthropogenic contamination as well.
PB  - Elsevier Science BV, Amsterdam
T2  - Talanta
T1  - Determination of metal content in some herbal drugs - Empirical and chemometric approach
VL  - 67
IS  - 1
SP  - 233
EP  - 239
DO  - 10.1016/j.talanta.2005.03.023
ER  - 
@article{
author = "Ražić, Slavica and Onjia, Antonije and Đogo-Mračević, Svetlana and Slavković, Latinka and Popović, Aleksandar",
year = "2005",
abstract = "The concentrations of Cu, Zn, Mn, Fe, K, Ca, Mg, Al, Ba and B in 26 herbal drugs of special importance in phytopharmacywere studied. Flame atomic absorption and emission spectrometry (FAAS, FAES), as well as inductively coupled plasma atomic emission spectrometry (ICP-AES), were applied in this work. The whole procedure, from sample preparation, via dissolution, to measurements, was validated by using CRM (NIST 1573a-tomato leaves), and the obtained recovery values are in the range from 91 to 102%. Drug samples originated from medicinal plants cultivated in Serbia contained Cu (4.47-14.08 mg kg(-1)), Zn (8.4-54.5 mg kg(-1)), Mn (9-155 mg kg(-1)), Fe (47-546 mg kg(-1)), K (0.20-6.24%), Ca (0.18-1.84%), Mg (0.13-1.09%), Al (16-416 mg kg(-1)), Ba (11.70-84.83 mg kg(-1)) and B (5.1-118.7 mg kg(-1)). In order to get a better insight into the elemental patterns, a common chemometric approach to data evaluation was used. Four significant factors identified by principal component analysis (PCA) were attributed partly to the significant influential sources and high mobility of some elements thus referring to potential anthropogenic contamination as well.",
publisher = "Elsevier Science BV, Amsterdam",
journal = "Talanta",
title = "Determination of metal content in some herbal drugs - Empirical and chemometric approach",
volume = "67",
number = "1",
pages = "233-239",
doi = "10.1016/j.talanta.2005.03.023"
}
Ražić, S., Onjia, A., Đogo-Mračević, S., Slavković, L.,& Popović, A.. (2005). Determination of metal content in some herbal drugs - Empirical and chemometric approach. in Talanta
Elsevier Science BV, Amsterdam., 67(1), 233-239.
https://doi.org/10.1016/j.talanta.2005.03.023
Ražić S, Onjia A, Đogo-Mračević S, Slavković L, Popović A. Determination of metal content in some herbal drugs - Empirical and chemometric approach. in Talanta. 2005;67(1):233-239.
doi:10.1016/j.talanta.2005.03.023 .
Ražić, Slavica, Onjia, Antonije, Đogo-Mračević, Svetlana, Slavković, Latinka, Popović, Aleksandar, "Determination of metal content in some herbal drugs - Empirical and chemometric approach" in Talanta, 67, no. 1 (2005):233-239,
https://doi.org/10.1016/j.talanta.2005.03.023 . .

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