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Development of a HPTLC method for in-process purity testing of pentoxifylline

Samo za registrovane korisnike
2005
Autori
Grozdanović, Olivera
Antić, Dušan
Agbaba, Danica
Članak u časopisu (Objavljena verzija)
Metapodaci
Prikaz svih podataka o dokumentu
Apstrakt
A HPTLC method for the separation and identification of pentoxifylline and related substances, impurities of reaction partners, and side reaction products has been developed using different mobile and stationary phases. For quantitative assay of possible by-products as impurities, LiChrosphere (R) RP-18 F254s chromatoplates, acetone-chloroform-toluene-dioxane (221:11 v/v) as a mobile phase, and detection at 275 nm were employed. Linearity (r >= 0.997), recovery (86.5-115.5%), and determination limit (0.1-0.6%) were evaluated and found to be satisfactory. This method enables monitoring of the synthesis, as well as purity control of pentoxifylline-containing raw materials and pharmaceuticals.
Ključne reči:
pentoxifylline / HPTLC / impurities / quantitation
Izvor:
Journal of Separation Science, 2005, 28, 6, 575-580
Izdavač:
  • Wiley-VCH Verlag GMBH, Weinheim

DOI: 10.1002/jssc.200400006

ISSN: 1615-9306

PubMed: 15881088

WoS: 000228760400011

Scopus: 2-s2.0-17844371309
[ Google Scholar ]
6
5
URI
http://farfar.pharmacy.bg.ac.rs/handle/123456789/587
Kolekcije
  • Radovi istraživača / Researchers’ publications
Institucija
Pharmacy

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