Micellar electrokinetic capillary chromatography determination of zinc bacitracin and nystatin in animal feed
Само за регистроване кориснике
2006
Чланак у часопису (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
An MEKC procedure was developed for the separation of zinc bacitracin (Zn-BC) and nystatin (NYS) in mixtures and in animal feedstuff. The running buffer was 15 mM borate/19 mM phosphate, pH 8.2, containing 20 mM SDS and 10% v/v methanol. Samples were run at 25 degrees C, the applied voltage was 25 IN, and an additional pressure of 5 mbar was applied. Both analytes were detected by LTV simultaneously at 215 nm, Zn-BC alone at 192 and 254 nm, and NYS alone at 305 nm. The method was shown to be specific, accurate (recoveries were 100.0 +/- 0.6% and 100.1 +/- 0.6% for Zn-BC and NYS, respectively), linear over the tested range (correlation coefficients 0.9991 and 0.9994), and precise (RSD below 1.3% for both analytes). The method was applied to determine Zn-BC and NYS as additives in animal feed.
Кључне речи:
animal feed additives / bacitracin / micellar electrokinetic capillary chromatography / nystatinИзвор:
Journal of Separation Science, 2006, 29, 9, 1288-1293Издавач:
- Wiley-VCH Verlag GMBH, Weinheim
DOI: 10.1002/jssc.200500477
ISSN: 1615-9306
PubMed: 16833088
WoS: 000238548300013
Scopus: 2-s2.0-33745470585
Институција/група
PharmacyTY - JOUR AU - Injac, Rade AU - Kac, Javor AU - Mlinarić, Ales AU - Karljiković-Rajić, Katarina PY - 2006 UR - https://farfar.pharmacy.bg.ac.rs/handle/123456789/825 AB - An MEKC procedure was developed for the separation of zinc bacitracin (Zn-BC) and nystatin (NYS) in mixtures and in animal feedstuff. The running buffer was 15 mM borate/19 mM phosphate, pH 8.2, containing 20 mM SDS and 10% v/v methanol. Samples were run at 25 degrees C, the applied voltage was 25 IN, and an additional pressure of 5 mbar was applied. Both analytes were detected by LTV simultaneously at 215 nm, Zn-BC alone at 192 and 254 nm, and NYS alone at 305 nm. The method was shown to be specific, accurate (recoveries were 100.0 +/- 0.6% and 100.1 +/- 0.6% for Zn-BC and NYS, respectively), linear over the tested range (correlation coefficients 0.9991 and 0.9994), and precise (RSD below 1.3% for both analytes). The method was applied to determine Zn-BC and NYS as additives in animal feed. PB - Wiley-VCH Verlag GMBH, Weinheim T2 - Journal of Separation Science T1 - Micellar electrokinetic capillary chromatography determination of zinc bacitracin and nystatin in animal feed VL - 29 IS - 9 SP - 1288 EP - 1293 DO - 10.1002/jssc.200500477 ER -
@article{ author = "Injac, Rade and Kac, Javor and Mlinarić, Ales and Karljiković-Rajić, Katarina", year = "2006", abstract = "An MEKC procedure was developed for the separation of zinc bacitracin (Zn-BC) and nystatin (NYS) in mixtures and in animal feedstuff. The running buffer was 15 mM borate/19 mM phosphate, pH 8.2, containing 20 mM SDS and 10% v/v methanol. Samples were run at 25 degrees C, the applied voltage was 25 IN, and an additional pressure of 5 mbar was applied. Both analytes were detected by LTV simultaneously at 215 nm, Zn-BC alone at 192 and 254 nm, and NYS alone at 305 nm. The method was shown to be specific, accurate (recoveries were 100.0 +/- 0.6% and 100.1 +/- 0.6% for Zn-BC and NYS, respectively), linear over the tested range (correlation coefficients 0.9991 and 0.9994), and precise (RSD below 1.3% for both analytes). The method was applied to determine Zn-BC and NYS as additives in animal feed.", publisher = "Wiley-VCH Verlag GMBH, Weinheim", journal = "Journal of Separation Science", title = "Micellar electrokinetic capillary chromatography determination of zinc bacitracin and nystatin in animal feed", volume = "29", number = "9", pages = "1288-1293", doi = "10.1002/jssc.200500477" }
Injac, R., Kac, J., Mlinarić, A.,& Karljiković-Rajić, K.. (2006). Micellar electrokinetic capillary chromatography determination of zinc bacitracin and nystatin in animal feed. in Journal of Separation Science Wiley-VCH Verlag GMBH, Weinheim., 29(9), 1288-1293. https://doi.org/10.1002/jssc.200500477
Injac R, Kac J, Mlinarić A, Karljiković-Rajić K. Micellar electrokinetic capillary chromatography determination of zinc bacitracin and nystatin in animal feed. in Journal of Separation Science. 2006;29(9):1288-1293. doi:10.1002/jssc.200500477 .
Injac, Rade, Kac, Javor, Mlinarić, Ales, Karljiković-Rajić, Katarina, "Micellar electrokinetic capillary chromatography determination of zinc bacitracin and nystatin in animal feed" in Journal of Separation Science, 29, no. 9 (2006):1288-1293, https://doi.org/10.1002/jssc.200500477 . .