Претраживање
Приказ резултата 61-70 од 77
Spectrophotometric determination of obidoxime chloride as its Pd(II) complex in water and injections
(Journal of Pharmaceutical and Biomedical Analysis, 1987)
It has been established that obidoxime chloride reacts with palladium(II) chloride in the pH range 3.9-8.0 and forms a yellow water-soluble (1:1) complex with maximum absorbance at 355 nm. By applying the methods of Sommer, ...
Application of experimental design in optimization of solid phase extraction of mycophenolic acid and mycophenolic acid glucuronide from human urine and plasma and SPE-RP-HPLC method validation
(Elsevier Science BV, Amsterdam, 2008)
The aim of this study was to develop and optimize a solid phase extraction (SPE) procedure for purification of mycophenolic acid (MPA) and its metabolite mycophenolic acid glucuronide (MPAG) in biological samples. During ...
Determination of paracetamol in pure and pharmaceutical dosage forms by pulse perturbation technique
(Elsevier Science BV, Amsterdam, 2006)
A new procedure for kinetic determination of paracetamol in pharmaceuticals is proposed. The method is based on potentiometric monitoring of the concentration perturbations of the matrix reaction system being in a stable ...
Acidity constants of cefetamet, cefotaxime and ceftriaxone; the effect of the substituent at C3 position
(Elsevier Science BV, Amsterdam, 2005)
Ionization constants of three cephalosporin antibiotics, cefetamet (CEF), cefotaxime (CFX) and ceftriaxone (CFTR) are determined using pH-potentiometric titrations at I= 0.1 M (NaCl) and t = 25 degrees C. Cefetarnet and ...
High-performance liquid chromatographic method for the determination of bumetanide in pharmaceutical preparations
(Journal of Pharmaceutical and Biomedical Analysis, 1989)
Use of palladium(II) chloride as colour-forming reagent in determination of pralidoxime chloride in water and tablets
(Journal of Pharmaceutical and Biomedical Analysis, 1988)
Pralidoxime chloride (PAM-2Cl) has been determined spectrophotometrically in Britton-Robinson buffer solution at pH = 6.45; the method is based on measurement of the absorbance of the Pd(II)-pralidoxime complex at 327 nm. ...
Densitometric determination of conjugated oestrogens in the raw material and in pharmaceutical preparations
(Journal of Pharmaceutical and Biomedical Analysis, 1990)
A densitometric method for determination of complex mixtures of conjugated oestrogens in raw material and tablets was developed. The proposed procedure comprised hydrolysis of sodium sulphate esters of oestrone, equilin, ...
Spectrophotometric determination of mesterolone in tablets using 3-acetylaminobenzaldehydethiosemicarbazone
(Journal of Pharmaceutical and Biomedical Analysis, 1989)
Quantitative analysis of analgoantipyretics in dosage form using planar chromatography
(Pergamon-Elsevier Science Ltd, Oxford, 2001)
In the therapy of pain of weaker genesis, frequently used drugs usually represent a mix of analgoantipyretics of different chemical structures, mostly derivatives of salicylic acid, pyrazolone and p-aminophenol as well as ...
Analytical method development supported by DoE-DS approach for enantioseparation of (S,S)- and (R,R)-moxifloxacin
(Elsevier B.V., 2023)
In this paper, method for enantiomeric purity testing of fourth-generation fluoroquinolone, moxifloxacin hydrochloride, was developed and validated. Exceptional enantioselectivity for this assay was achieved using cyclodextrin ...