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Densitometric determination of conjugated oestrogens in the raw material and in pharmaceutical preparations
(Journal of Pharmaceutical and Biomedical Analysis, 1990)
A densitometric method for determination of complex mixtures of conjugated oestrogens in raw material and tablets was developed. The proposed procedure comprised hydrolysis of sodium sulphate esters of oestrone, equilin, ...
Potentiometric investigation of the stability of palladium(II) complex of pralidoxime chloride in aqueous solution
(Journal of Pharmaceutical and Biomedical Analysis, 1990)
The formation of a complex between palladium(II) chloride and pralidoxime chloride (PAM-2Cl) has been studied by means of potentiometric pH measurements. The real stability constant of the complex in aqueous medium of ionic ...
Spectrophotometric investigation of complex formation of an oxime PAM-4Cl with palladium(II) and its analytical application
(Journal of Pharmaceutical and Biomedical Analysis, 1990)
The colour reaction of 4-hydroxyiminomethyl-1-methylpyridinium chloride (PAM-4Cl) and palladium(II) chloride has been investigated. The optimum reaction conditions, spectral characteristics, conditional stability constant ...
Gas chromatography mass spectrometry determination of isosorbide 5-mononitrate and related impurities in raw materials and dosage formulations
(Pergamon-Elsevier Science Ltd, Oxford, 1997)
A straightforward quantitative method for gas chromatography-mass spectrometry determination of isosorbide 5-mononitrate (ISSMN) and its related impurities such as isosorbide (IS), isosorbide diacetate (ISDA) and isosorbide ...
Spectrophotometric determination of desoximetasone in ointment using 1,4-dihydrazinophthalazine
(Pergamon-Elsevier Science Ltd, Oxford, 1996)
The proposed method is based on coloured hydrazone formation with 1,4-dihydrazinophthalazine as a reagent. Heating at 85 degrees C for 2 h was found necessary to ensure optimal hydrazone formation in the presence of ...
Application of artificial neural networks in HPLC method development
(Pergamon-Elsevier Science Ltd, Oxford, 1998)
The use of artificial neural networks (ANNs) for response surface modelling in HPLC method development for amiloride and methychlothiazide separation is reported. The independent input variables were pH and methanol ...
Densitometric determination of metoprolol tartrate in pharmaceutical dosage forms
(Pergamon-Elsevier Science Ltd, Oxford, 1997)
This paper describes a simple densitometric method for the determination of metroprolol tartrate in tablets and ampoules. After separation on silica gel GF254 plates, using acetone-methanol-triethylamine as the mobile phase ...
Spectrophotometric determination of nizatidine in pharmaceutical formulations
(Journal of Pharmaceutical and Biomedical Analysis, 1995)
Coulometric determination of nizatidine
(Journal of Pharmaceutical and Biomedical Analysis, 1995)
Coulometric determination of some antiasthmatics
(Journal of Pharmaceutical and Biomedical Analysis, 1993)
A simple and rapid method for the assay of microquantities of fenoterol hydrobromide, orciprenaline sulphate and terbutaline sulphate in pure state and various pharmaceutical formulations, is presented. The method is based ...